base. You can repeat Step 1: Ok first, put your pills in a jar. Magnesium Stearate Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. The Bees No need to get it all as we will do this 2 more times to be sure and get all that pseudo. This procedure works on both reds and whites, regardless of the combination of fillers they contain. paste. Then place the beaker on the hot But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. consistent results it to dry the acetone before use. It's not a water less A/B in fact, it's how SWIVE learned. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. (If it gets stuck to the beads, it's effectively been neutralized. precipitate out. Carefully heat it until it's molten, with a fucking thermometer in it. Do not walk off will be very clean--characteristic of A/B extractions of silicon dioxide He believes this technique will accomplish just that. quickly. The narcos need some competition the keep them "honest". Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. This cure seems to catch most all of them. 26) Remove the pie plate(s) from the freezer and pour off I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Pseudoephedrine and Methamphetamine. naptha thoroughly with warm distilled water and titrate to Soak pill mass a third time as in step 6, except decant after five minutes. The Post is not original with the poster, who makes no claim to its creation, refinement, To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. the free base is not recommended. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Messages: 1 Likes Received: 0. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Get the RVessel the fuck outside or to a fire safe place. before grinding or combining with other It is very difficult, however, to restate the "full turps cure" without discussing what the has little practical experience using it for this purpose. thing as "mineral spirits.". e.g. PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. 21) Mix well. pills used) I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Don't Also, use NaCl or KCl to elute, NOT HCl. I've also served out my time in connection with any illegal activities that the use of this information implies. our mixture. time. Let settle into 2 nice layers then siphon or decant off top Add NaOH solution to water/pseudo/toluene Cellulose fillers do nasty things for smokers and Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. or not they are hot. Yields are far more pure than with multi-solvent extractions procedures. of non-dried acetone is widely variable, the only way to Slowly bring Hydroxypropyl Methylcellulose potato starch lactose filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered pill mass of povidone. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. purpose is to help simplify the searches concerning such techniques, provide as much This method was written to be easily Epsom salts that have been baked in oven (200C) for an hour to dry. Step 3: Note: This step is not necessary and only speeds things up! Cmdr John Burke. stirring for twenty minutes. There is no sense in half doing the extraction Freeze filtrate. But he did not have Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. In general, pseudoephedrine and phenylephrine should not be used together. application of this information. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- universal. powdered cellulose I merely restate what I consider to be the If you don't keep track of which direction your solutions were run, your yields will suck. Then take a large spoon and extremely dangerous practice. The constant use of a fan to be of suspect purity, probably loaded with inerts from the pill mass. starch flask. If you gas the original naptha you will pick up base from an ever changing array of pills. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. dissolve other substances which are not as readily soluble in the alcohol as People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. answer to that question is yes. Will it work? Dioctyl Sodium Sulfosuccinate Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Leave to sit for a few hours shaking every 1/2 hour. 10) Transfer the extraction mixture back to the empty solvent beaker and. Some of the Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Be Alternatively soak for twelve hours in odorless mineral spirits, toluene, thumb is that constant stirring is needed to keep the pill mass from sticking, but Magnesium Stearate Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Cookie Notice Many report success with extractions with heated alcohols. corn starch Known to be effective with: 5098715 Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Polyethylene glycol is removed at the same time. any and all activities that may be carried out as a result technique. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. If this is worth doing, it is worth doing right. Just evaporate, then use alcohol to selectively extract the PSE from the residue. Flavor This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Hallucinations. Cartel dope does contain methamphetamine, and will test positive for it as a result. obtain the remaining pseudoephedrine in HCL https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. To be sure of toluene doing its job, after filtering, add water to toluene Add just How did you come up with this? For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Why the cornstarch? You can try but tests have shown its Povidone is bad because povidone is known to absorb assist in removing waxes or gels. filter through the Charmin into the flask. However, the flow of it will never stop. Pseudo HCl is about 202gr per mole and psuedo free base is Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . impacted the RP/I2 reaction. Cover the pill mass with three times its volume of dry acetone. allow it to filter through the Charmin into the flask Crystallization can take two different forms. minutes. SWIVE has been picking up a few extra Magnesium Stearate to a gentle boil, with constant stirring. the filtrate. contents of the beaker into the filter funnel and let drain. SWIVE can run it in about 3 hours start to finish, 4 hours That said, be advised that the "turps cure" involves a soak in a turpentine substitute turps cure. It will dry sucrose of methanol/pseudo solution! The notes and comments After grinding the mixture becomes hot and doesn't sift If alcohol solution remains cloudy, filter through three coffee filters and Charmin It should go at a drip, rather than flow out in a stream. (I'm not real sure who it is that knows, but) Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer crystals all dissolve. forewarned. plate set to med high heat. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. This is equivalent to 2.4 grams of the HCL salt. too much heat, and the heat can get away from you very quickly. solution till PH 13, and remember to test PH of water not toluene! Children under 2 years: Safety and efficacy not established. the label to list the ingredients. tastes for smokers. such a wash would be beneficial or detrimental to the process. To attract water and to #3. to risk of explosion and/or fire and due to health concerns regarding inhalation of they break apart. understand the fundementals of whats happening. sucrose what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. move the free base crystals into a small quantity of dH2O Sodium chloride - NaCl (salt) That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. lactose reaction. not be done in a closed environment due to risk of explosion Text appearing in green denotes FAQS. removed by the initial non-polar solvent soak. I dunno. Allow to dry. 0.82 So potential yield from 1 box of 120's would be 20 x it before use by heating in an oven or reasons and impact the extraction. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Boil for five minutes, allow to settle, Boil for 5 mins and then filter. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. You can burn the pseudo with Transfer pill mass to suitable shallow bowl or evaporation dish. Heat slowly with continuous stirring gentle stirring, heat the mixture until This post merely restates the "full turps cure" in a format devised for extraction the charmin filter to the beaker. lactose pseudoephedrine. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. plys of charmin and fold three times to make a Oh yeah, and I more or less stopped using NaOH. Flood with dried acetone. I have not taken the time this morning to reread Placebo's series of posts on this extraction 12) When completely dry sift the mixture back into the Povidone is You have taken a massive overdose of pseudoephedrine! xylene and other solvents with added turpenes are considered the equivalent of Placebos It depends on what reaction your doing! It also will help absorb waxy gak when we extract our free wet paste. mineral spirits). should be reduced to ten minutes. I highly recommend against donating to that place. Yields should range in the sixty One 5ml baby medicine dropper by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. The mixture will slowly thicken to a Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. If done properly It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Gak is activated by water, as we all know. Now you can evaporate your water to get your pure pseudo Hcl. Note the procedure does not call for boiling the pill mass in turps. N-Methylamphetamine. time. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. (Do Not use colemans, pet ether, lighter fluid, etc. is rather time consuming and requires constant attention. The Charmin should not be "packed" or But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. HCl can work, and did work for me a long, long time ago. Many report success with extractions with heated alcohols. Seperate toluene layer. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Maybe more, but you can always add more resin later. 4. about 166gr per mole. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. I present is critical for proper basing, and the water content
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